4a | 5a | 6a | 7b | 8a | 9b | 10b | |||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
H | δH (J in Hz) | δH (J in Hz) | δH (J in Hz) | δH (J in Hz) | δH (J in Hz) | δH (J in Hz) | δH (J in Hz) | ||||||||
1 | 1.67 m, 2.71 m | 1.28 m, 1.95 m | 1.25 m, 1.96 m | 1.38 m, 2.11 m | 1.42 m, 1.99 m | 1.82 m, 2.77 m | 1.80 t (13.1), 2.53 m | ||||||||
2 | 2.60 m, 2.96 m | 2.60 m, 2.88 m | 2.43 ddd (14.3, 8.1, 6.8), 2.70 ddd (14.2, 8.6, 5.9) | 2.43 ddd (14.1, 8.4, 6.0), 2.77 m | 2.58 dd (13.2, 5.1), 2.89 td (13.3, 7.0) | 2.74 m, 3.00 m | 2.70 m, 2.95 m | ||||||||
3 | - | - | - | - | - | - | - | ||||||||
4 | - | - | - | - | - | - | - | ||||||||
5 | 2.37 d (8.4) | 2.40 d (9.3) | 2.18 d (9.7) | 2.29 d (9.8) | 2.44 d (9.3) | 2.45 d (8.3) | 2.78 d (9.7) | ||||||||
6 | 4.05 dd (12.7, 5.6) | 3.66 m | 3.64 m | 3.70 dd (9.9, 4.9) | 3.70 m | 4.10 m | 3.64 m | ||||||||
7 | 1.58 m, 1.79 m | 1.51 m, 1.69 m | 1.58 m, 1.71 m | 1.75 (2 H) | 1.62 m, 1.70 m | 1.72 m, 1.85 m | 1.65 m, 1.90 m | ||||||||
8 | 1.59 m | 1.72 m | 1.86 m | 1.88 m | 1.72 m | 1.67 m | 1.94 m | ||||||||
9 | - | - | - | - | - | - | - | ||||||||
10 | - | - | - | - | - | - | - | ||||||||
11 | 1.15 m, 2.30 m | 0.80 m, 2.02 m | 0.91 m, 1.98 m | 1.76 m, 2.38 m | 1.67 m, 2.35 dd (14.6, 5.8) | 2.04 dd (14.5, 8.4), 2.69 dd (14.5, 6.8) | 2.11 m, 2.73 m | ||||||||
12 | 1.68 m, 1.84 m | 1.74 m, 1.85 m | 1.69 m, 1.82 m | 4.26 ddd (9.2, 6.1, 2.6) | 4.25 t (7.6) | 4.28 t (7.9) | 4.28 t (7.7) | ||||||||
13 | - | - | - | - | - | - | - | ||||||||
14 | - | - | - | - | - | - | - | ||||||||
15 | 1.77 m, 2.15 m | 1.80 m, 2.15 m | 1.79 m, 2.17 m | 1.90 m, 2.19 dd (12.7, 7.9) | 1.89 m, 2.21 dd (12.5, 7.8) | 1.89 m, 2.23 dd (12.6, 7.7) | 1.91 m, 2.21 dd (12.6, 7.9) | ||||||||
16 | 4.89 dd (13.4, 7.7) | 4.68 dt (8.2, 4.2) | 4.90 tdd (8.1, 5.4, 3.2) | 4.93 m | 4.93 m | 4.93 q (7.2) | 4.94 m | ||||||||
17 | 2.06 d (7.7) | 2.10 d (7.7) | 2.07 d (7.3) | 2.97 d (8.0) | 2.96 d (8.1) | 2.97 d (8.3) | 2.99 d (8.0) | ||||||||
18 | 1.71 s | 1.70 s | 1.68 s | 1.71 s | 1.70 s | 1.76 s | 1.75 s | ||||||||
19 | 0.59 d (4.4), 1.00 d (4.4) | 0.53 d (5.0), 0.79 d (4.9) | 0.31 d (4.1), 0.64 d (4.2) | 0.48 d (4.2), 0.70 d (4.2) | 0.67 d (4.8), 0.84 d (4.9) | 0.74 d (4.4), 1.06 d (4.4) | 0.63 d (4.4), 0.73 d (4.4) | ||||||||
20 | - | - | - | - | - | - | - | ||||||||
21 | 1.55 s | 1.60 s | 1.57 s | 1.99 s | 1.97 s | 1.98 s | 1.99 s | ||||||||
22 | 1.24 m, 3.03 m | 1.26 m, 3.11 m | 1.24 m, 3.08 td (13.5, 4.5) | 2.13 dd (13.1, 3.7) | 2.10 d (13.4), 2.78 t (12.2) | 2.13 m, 2.78 m | 2.13 m, 2.81 m | ||||||||
23 | 1.87 m, 2.16 m | 1.91 m, 2.21 m | 1.87 m, 2.19 m | 1.94 dd (14.0, 3.7), 2.34 t (3.4) | 1.95 m, 2.35 m | 1.93 m, 2.34 t (13.9) | 1.94 m, 2.34 t (14.0) | ||||||||
24 | 3.66 brs | 3.70 brs | 3.66 brs | 3.73 brs | 3.72 brs | 3.73 brs | 3.74 s | ||||||||
25 | - | - | - | - | - | - | - | ||||||||
26 | 1.44 s | 1.47 s | 1.44 s | 1.57 s | 1.56 s | 1.58 s | 1.59 s | ||||||||
27 | 1.27 s | 1.32 s | 1.28 s | 1.39 s | 1.39 s | 1.40 s | 1.40 s | ||||||||
28 | 1.76 s | 1.93 s | 1.74 s | 1.78 s | 1.94 s | 1.80 s | 5.09 s, 5.21 s | ||||||||
29 | 1.60 s | 1.67 s | 1.42 s | 1.50 s | 1.70 s | 1.65 s | 1.89 s | ||||||||
30 | 0.94 s | 0.94 s | 0.92 s | 1.28 s | 1.27 s | 1.31 s | 1.33 s |